HCID 13935137, compound → 104628-33-3

HRID 1763046Notes

Reaction equation

HRID 1763046 reaction equation
[Cl:1][C:2]1[CH:24]=[CH:23][C:5]([CH2:6][NH:7][C:8]2[C:9]3[C:14]([N:15]=[C:16]4[C:21]=2[C:20](=[O:22])[CH2:19][CH2:18][CH2:17]4)=[CH:13][CH:12]=[CH:11][CH:10]=3)=[CH:4][CH:3]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>O1CCCC1>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][NH:7][C:8]2[C:9]3[C:14]([N:15]=[C:16]4[C:21]=2[CH:20]([OH:22])[CH2:19][CH2:18][CH2:17]4)=[CH:13][CH:12]=[CH:11][CH:10]=3)=[CH:23][CH:24]=1

Participants

4

Reactant 2

HCID 13935137HCID 13935137, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 3025623104628-33-3

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent2×

Procedure

To a cooled solution of 6.25 g of 9-(4-chlorobenzylamino)-3,4-dihydroacridin-1(2H)-one in 140 ml of tetrahydrofuran was added 10 ml of 1M LiAlH4 solution in THF. This was stirred at ice bath temperature for 1 hour.

Sources & evidence

ORD record
ord-cd9aab54ac2d442b815c94c39056bc8f
Source dataset
uspto-grants-1989_05
Patent number
US04835275

Reaction notes

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