Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | tert-Butyl mercaptan | HCID 6387 | — |
| Reactant | 1,3,5-Trimethyl-1,3,5-triazacyclohexane | HCID 7952 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20309108 | HCID 20309108 | — |
Reaction Steps
Two hundred ml. of acetonitrile and 6.45 g. (0.05 mole) of 1,3,5-trimethylhexahydro-s-triazine are charged to a 500 ml. 3-neck round bottom flask equipped with a stirrer, thermometer and dropping funnel. The mixture is stirred and cooled to -30° C. with a dry ice/acetone bath. Six grams of hydrogen chloride gas are added, followed by slow addition of 13.5 g. (0.15 mole) of tert.-butyl mercaptan dissolved in 50 ml. of acetonitrile. The mixture is then allowed to warm to room temperature and stand overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04111682 |
|---|
| Source dataset | uspto-grants-1978_09 |
|---|
| ORD ID | ord-5246002422484162be2eb192c1c5b48a |
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| Source note | uspto-grants-1978_09 |
|---|
