HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N,N'-dimethylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N-methylurea | HCID 20534526 | — |
| Product | N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N,N'-dimethylurea | HCID 22768164 | — |
Reaction Steps
The reaction is effected as in Example 171 by using 1-methyl-1-butyl-3-(5-t-butyl-3-isoxazolyl)urea and methyl iodide to give 1,3-dimethyl-1-butyl-3-(5-t-butyl-3-isoxazolyl)urea as an oil boiling at 130° to 135° C. (bath temperature)/0.25 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04111680 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-f432c8a560c340b1b1c7467db15b7b34 |
| Source note | uspto-grants-1978_09 |