HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20310367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-(3-Chlorophenyl)-2-methyl-4-oxobutanoic acid | HCID 587354 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20310367 | HCID 20310367 | — |
Reaction Steps
A mixture of 7.11 g. of 3-(m-chlorobenzoyl)-2-methylpropionic acid, 50 ml. of ethanol and 3.0 ml. of hydrazine hydrate is refluxed for 2 hrs. Cooling and filtering gives crystals, (m.p. 150°-151° C.) which are recrystallized from ethanol to give 5.72 g. of crystals, m.p. 152°-153°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-42a48005974145e5a29d6b0ca72cd92f |
| Source note | uspto-grants-1978_09 |