HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → 3-(3-Chlorophenyl)-6-hydrazinylpyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 3-Chloro-6-(3-chlorophenyl)pyridazine | HCID 12726811 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Product | 3-(3-Chlorophenyl)-6-hydrazinylpyridazine | HCID 13388909 | — |
Reaction Steps
A mixture of 6.85 g of 3-chloro-6-(m-chlorophenyl)pyridazine, 100 ml. of n-butanol and 3.05 g. of hydrazine hydrate is refluxed overnight. The solvent is removed under vacuum to give a semi-solid. The solid is dissolved in a minimum of hot nitromethane. Cooling gives 3.5 g. of amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-44d2a40e22344964a98de9946f60179e |
| Source note | uspto-grants-1978_09 |