HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetohydrazide → HCID 12726849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetohydrazide | HCID 14039 | — |
| Reactant | HCID 12449558 | HCID 12449558 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 12726849 | HCID 12726849 | — |
Reaction Steps
As in Example 36, a mixture of 8.0 g. of 3-chloro-4-methyl-6-(α,α,α-trifluoro-m-tolyl)pyridazine, 4.34 g. of acetylhydrazine in 125 ml. of n-butanol is refluxed for 48 hrs. to give 3.9 g. of product as crystals, m.p. 196°-198° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-1cc5603c4d5f45a08b237b971efe3735 |
| Source note | uspto-grants-1978_09 |