1-Butanol → HCID 12726837, compound

HRID 1763613Notes

Reaction equation

HRID 1763613 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:9]=[C:10]([CH3:14])[CH:11]=[CH:12][CH:13]=2)=[CH:6][CH:7]=1.[CH:15]([NH:17][NH2:18])=O.C(O)CCC>C(Cl)(Cl)Cl.CCCCCC>[C:10]1([CH3:14])[CH:11]=[CH:12][CH:13]=[C:8]([C:5]2[CH:6]=[CH:7][C:2]3[N:3]([CH:15]=[N:17][N:18]=3)[N:4]=2)[CH:9]=1

Participants

5

Reactant 3

HCID 2631-ButanolHCID 12229HydrazinecarboxaldehydeHCID 124495613-Chloro-6-(3-methylphenyl)pyridazine

Product 1

HCID 12726837HCID 12726837, compound

Reagents, catalysts & solvents 1

HCID 21585165Chloroform hexaneSolvent

Procedure

A mixture of 6.0 g of 3-chloro-6-(m-tolyl)pyridazine and 3.52 g of formylhydrazine in 100 ml. of n-butanol is refluxed for 48 hrs. and worked up as in Example 35 to give 2.0 g. of white crystals (from CHCl3 -hexane), m.p. 164°-166° C.

Workup

  1. customto give 2.0 g

Sources & evidence

ORD record
ord-b3fa8f44218b43ffbded77a1d84e9aee
Source dataset
uspto-grants-1978_09
Patent number
US04112095

Reaction notes

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