HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 12726837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Hydrazinecarboxaldehyde | HCID 12229 | — |
| Reactant | 3-Chloro-6-(3-methylphenyl)pyridazine | HCID 12449561 | — |
| Solvent | Chloroform hexane | HCID 21585165 | — |
| Product | HCID 12726837 | HCID 12726837 | — |
Reaction Steps
A mixture of 6.0 g of 3-chloro-6-(m-tolyl)pyridazine and 3.52 g of formylhydrazine in 100 ml. of n-butanol is refluxed for 48 hrs. and worked up as in Example 35 to give 2.0 g. of white crystals (from CHCl3 -hexane), m.p. 164°-166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-b3fa8f44218b43ffbded77a1d84e9aee |
| Source note | uspto-grants-1978_09 |