HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde → HCID 20310359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde | HCID 12229 | — |
| Reactant | 5-Chloro-2-methylbenzaldehyde | HCID 12347565 | — |
| Reactant | HCID 20310362 | HCID 20310362 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20310359 | HCID 20310359 | — |
Reaction Steps
As described in Example 35, 2-methyl-5-chlorobenzaldehyde is converted to 3-chloro-6-(2-methyl-5-chlorophenyl)pyridazine. A mixture of the preceding compound and formylhydrazine in n-butanol is refluxed for 24 hours to give the product of the example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-22ff91238a354d2bb2b52a9689da92bd |
| Source note | uspto-grants-1978_09 |