HCID 54043940, compound → HCID 20310965, compound

Participants

Reaction Steps

m-[N-(4-Hydroxynonyl)methanesulfonamidomethyl]-cinnamic acid (3.0 g., 0.075 mole) dissolved in ethanol (80 ml.) is hydrogenated over 0.8 g. of a 5% Pd on charcoal catalyst at one atmosphere of pressure and room temperature. After the theoretical amount of hydrogen is absorbed, the catalyst is removed by filtration. The ethanol is evaporated and the residual solid is purified by crystallization to afford the pure title compound.

Provenance & Evidence