HRID1763730

反应详情

EQUATION

反应方程式

HRID 1763730 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 1.95 g. of Nα -benzyloxycarbonyl-D-leucyl-L-leucine methyl ester in 50 ml. of absolute methanol containing 2.08 ml. of 2.38N hydrogen chloride in methanol is treated with 250 mg. of 10% palladium on carbon and is shaken in a hydrogen atmosphere until thin layer chromatography of solution samples indicate completion of the reaction. The catalyst is removed by filtration and the filtrate taken to dryness. The product is used without further purification.

WORKUP

后处理

  1. customcompletion of the reaction
  2. customThe catalyst is removed by filtration
  3. customThe product is used without further purification