Potassium Iodide → HCID 86736004, compound

Participants

Reaction Steps

62 g of 1,1,3-trichloro-propene, prepared according as described in Example 1, were reacted with 36.6 g of potassium adipate for 6 hours at 135° C. in the presence of 2 g of triethylamine and 0.3 g of potassium iodide. The reaction product was then washed and freed of the low-boiling components by means of distillation under vacuum. By a successive molecular distillation (120° C./10-4 mm Hg) 47 g of a substance were obtained which on elementary analysis showed the following composition:

Provenance & Evidence