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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1763901Generated: October 31, 2026

Tetrafluoro-m-phenylenediamine dihydrochloride → HCID 44522644, compound

https://huagongshe.com/reaction/1763901

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrafluoro-m-phenylenediamine dihydrochlorideHCID 149026—
ReactantHCID 15113388HCID 15113388—
ReactantHCID 20308544HCID 20308544—
SolventWaterHCID 962—
ProductHCID 44522644HCID 44522644—

Reaction Steps

The title compound was prepared from (+)- 7 -methoxy- 2 -methyl- 4 -phenyl- 1,2,3,4 -terahydro isoquinoline via (+)- 7 -hydroxy- 2 -methyl- 4 -phenyl- 1,2,3,4 -tetrahydro isoquinoline which was characterised as its hydrochloride salt m.p. 222°-3° C. (methanol-ether) [α]D25 + 24.1° (water) by the method of Example 1. The title compound was characterised as its dihydrochloride salt m.p. 160°-4° (hydroscopic) (ethanol ethyl acetate), [α]D5 + 13° (water). -tetrahydro

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04113869
Source datasetuspto-grants-1978_09
ORD IDord-3151a928cca449b2a87425ee5be34f54
Source noteuspto-grants-1978_09