HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoro-m-phenylenediamine dihydrochloride → HCID 44522644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | HCID 15113388 | HCID 15113388 | — |
| Reactant | HCID 20308544 | HCID 20308544 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 44522644 | HCID 44522644 | — |
Reaction Steps
The title compound was prepared from (+)- 7 -methoxy- 2 -methyl- 4 -phenyl- 1,2,3,4 -terahydro isoquinoline via (+)- 7 -hydroxy- 2 -methyl- 4 -phenyl- 1,2,3,4 -tetrahydro isoquinoline which was characterised as its hydrochloride salt m.p. 222°-3° C. (methanol-ether) [α]D25 + 24.1° (water) by the method of Example 1. The title compound was characterised as its dihydrochloride salt m.p. 160°-4° (hydroscopic) (ethanol ethyl acetate), [α]D5 + 13° (water). -tetrahydro
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04113869 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-3151a928cca449b2a87425ee5be34f54 |
| Source note | uspto-grants-1978_09 |