Hydrogen Bromide → HCID 20308591, compound

Participants

Reaction Steps

To a solution of 2-aminomethyl-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate (65 mg., 0.16 millimole) in ethanol (2 ml.) is added slowly with stirring 48% hydrobromic acid (0.5 ml.) at 20° C. After standing at 20° C. for 15 minutes, the deposited solid is collected and dried to give 2-aminomethyl-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate hydrobromide as a colorless solid (70 mg., 89%), m.p. 243°-244° C. with dec.

Provenance & Evidence