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HRID1764

反应详情

EQUATION

反应方程式

HRID 1764 的结构方程式

REACTANTS

反应物

2
结构：CSC
HCID1068

Dimethyl sulfide

C2H6S

结构：CCOC(=O)CBr
HCID7748

Ethyl bromoacetate

C4H7BrO2

PRODUCTS

生成物

1
结构：CCOC(=O)C[S+](C)C.[Br-]
HCID78861

(2-Ethoxy-2-oxoethyl)(dimethyl)sulfanium bromide

C6H13BrO2S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88°-90° C.