HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → HCID 14876357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | HCID 22770068 | HCID 22770068 | — |
| Product | HCID 14876357 | HCID 14876357 | 54.1% |
Reaction Steps
20.4 g of 2-methyl-5-propargyloxybenzothiazole and 12.5 g of propargyl bromide were heated on a hot water bath at 80° to 100° C for 3 hours. The precipitated crystals were washed with acetone to give 17.5 g of 2-methyl-3-propargyl-5-propargyloxybenzothiazolium bromide, m.p. 244° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04115122 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-1c216a920bf640dba0199f66d56e717c |
| Source note | uspto-grants-1978_09 |