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HRID1764097

反应详情

EQUATION

反应方程式

HRID 1764097 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

2 次

结构：Cc1nn(C)c2nc(-c3ccccc3)cc(N(C)C)c12
HCID22770498

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nn(C)c2nc(-c3ccccc3)cc(N(C)C)c12.Cl
HCID22770497

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

To 16.5 gms. of 4-dimethylamino-1,3-dimethyl-6-phenyl-1H-pyrazolo[3,4-b]pyridine (0.062 mol.) dissolved in 250 ml. of absolute ethanol, 10.7 ml. of ethereal hydrochloric acid (228 gms/1) are added. The solution is allowed to crystallize overnight to obtain 17.2 gms. (91%) of the hydrochloride, m.p. 219°-220° C. (dec.)

WORKUP

后处理

  1. customto crystallize overnight
  2. customto obtain 17.2 gms