HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → alpha-[p-(1-Cycloheptenyl)-phenoxy]-octanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | alpha-[p-(1-Cycloheptenyl)-phenoxy]-octanoic acid ethyl ester | HCID 53940125 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | alpha-[p-(1-Cycloheptenyl)-phenoxy]-octanoic acid | HCID 20306764 | — |
Reaction Steps
Analogously to the process described in Example 2, 13 g of α-[p-(1-cycloheptenyl)-phenoxy]-octanoic acid ethyl ester, on alkaline saponification with 27 ml of 2 N sodium hydroxide solution in 130 ml of ethanol, give α-[p-(1-cycloheptenyl)-phenoxy]-octanoic acid of melting point 59°-60° C (from cold hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04115416 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-7c871aad059e4a99a7ed5736870f3981 |
| Source note | uspto-grants-1978_09 |