HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 22768169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | 3-Isocyanato-5-methyl-1,2-oxazole | HCID 22768166 | — |
| Product | HCID 22768169 | HCID 22768169 | — |
Reaction Steps
To a suspension of 5-methyl-3-isoxazolyl isocyanate (1.71 g) in benzene (46 ml), allyl alcohol (0.88 g) is added, and the resultant mixture is refluxed for 3 hours. After cooling, the reaction mixture is evaporated to remove the solvent, whereby allyl N-(5-methyl-3-isoxazolyl)carbamate (2.38 g) is obtained. This substance is recrystallized from cyclohexane to give crystals melting at 76.5° to 77.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04116671 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-ff552b5166fe4a0680e4cc02b52552fe |
| Source note | uspto-grants-1978_09 |