HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1764426Generated: November 1, 2026
2-Propen-1-amine, acetate → HCID 136388423, compound
https://huagongshe.com/reaction/1764426
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Propen-1-amine, acetate | HCID 12203658 | — |
| Reactant | 6-Methyl-2-(methylsulfanyl)-5-propylpyrimidin-4(1H)-one | HCID 135735592 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 136388423 | HCID 136388423 | — |
Reaction Steps
A mixture of allylamine acetate (12 g) and 6-methyl-2-methylthio-5-propylpyrimid-4(3H)-one (6 g) was heated at 130° C for 45 minutes. The mixture was cooled and water was added. The precipitated product was collected, washed with water, dried and recrystallised from petroleum (b.p. 80°-100° C) giving 2-allylamino-6-methyl-5-propylpyrimid-4(3H)-one (formula VII, R1 = CH3, R = C3H7, R6 = H, R7 = CH2CH=CH2) having a melting point of 152°-153° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04116674 |
|---|
| Source dataset | uspto-grants-1978_09 |
|---|
| ORD ID | ord-a62dc830bb78446a90f7b1808986b1be |
|---|
| Source note | uspto-grants-1978_09 |
|---|
