Acetone → HCID 21820147, compound

Participants

Reaction Steps

A solution of 0.4 g of sodium hydroxide in 4 ml of water was added dropwise with stirring over a period of 20 minutes to a solution of 1.93 g of 2-ethylamino-4,6-dichlorotriazine and 1.85 g of cyanuric chloride in 50 cc of acetone which had been cooled to 0°-5° C. Stirring was continued for 6 hours after all the sodium hydroxide solution had been added. The resulting solution was then neutralised with sodium carbonate and stirred into ice water. The precipitate was collected, dried and recrystallised from ligroin.

Provenance & Evidence