HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22769263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 22769179 | HCID 22769179 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22769263 | HCID 22769263 | — |
Reaction Steps
0.1 mol (29.9 g) of 3-methyl-4-phenyl-1-(p-chlorobenzyl)-5-pyrazolone were dissolved in 400 ml of absolute dioxane. After adding 15 ml of triethylamine, 0.11 mol (17.6 g) of 4-chlorobenzoyl chloride in dioxane was added dropwise. After heating for several hours under reflux, the reaction batch was worked up as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04117143 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-59a8a978602844e2905d7b84c2d24962 |
| Source note | uspto-grants-1978_09 |