HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 22769768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Benzene, 1,1'-((methylsulfonyl)methylene)bis(4-chloro- | HCID 101397 | — |
| Product | HCID 22769768 | HCID 22769768 | — |
Reaction Steps
The procedure for making bis(p-chlorophenyl)methyl methyl sulfone was followed, using a slight excess of m-chloroperbenzoic acid (0.027 mole acid to 0.025 mole of bis(p-chlorophenyl)methyl n-butyl sulfoxide). A light amber liquid was formed and this gave crystals which were recrystallized from methanol as a white solid of bis(p-chlorophenyl)methyl n-butyl sulfoxide, melting point 116°-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04117168 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-8c78460f39714bbbba2905a15c2cf900 |
| Source note | uspto-grants-1978_09 |