Hydrazine hydrate (1:1) → HCID 22769787, compound

HRID 1764750Notes

Reaction equation

HRID 1764750 reaction equation
C([CH:3]([N:7]([CH:21](CC)[C:22]([O-:24])=O)[CH:8]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[C:4]([O-])=[O:5])C.O.[NH2:28][NH2:29]>CO>[C:9]1([CH:8]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[N:7]2[CH2:21][C:22](=[O:24])[NH:29][NH:28][C:4](=[O:5])[CH2:3]2)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 131711267HCID 131711267, compound

Product 1

HCID 22769787HCID 22769787, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Reacting diethyl-N-benzhydryliminodiacetate with hydrazine hydrate in the presence of methanol at reflux temperature and a reaction time of 20 hours to afford 5-diphenylmethyl-3,7-diketo-1,2-dihydro-1,2,5-triazepine.

Workup

  1. temperatureat reflux temperature

Sources & evidence

ORD record
ord-274b9acff752489ea24463491e0fcd62
Source dataset
uspto-grants-1978_09
Patent number
US04117225

Reaction notes

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