HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23115712, compound → 1-(3-Hydroxy-1-hexyl)-2,3,4-trifluorobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23115712 | HCID 23115712 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(3-Hydroxy-1-hexyl)-2,3,4-trifluorobenzene | HCID 23115709 | — |
Reaction Steps
After 1-(3-hydroxy-1-hexynyl)-2,3,4-trifluorobenzene was dissolved in ethanol, 5% palladium carbon (50% in water) was added thereto, and stirred for 6 hours at a hydrogen pressure of 0.5 MPa, and the mixture was left to stand overnight. After palladium carbon was removed by filtration, the solvent was evaporated under a reduced pressure to obtain 1-(3-hydroxy-1-hexyl)-2,3,4-trifluorobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226644B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-df9f7b75b88247ce807619c06e8e164f |
| Source note | uspto-grants-2007_06 |