HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → HCID 22732377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | 4-chloro-6-methyl-2-(3-methylphenyl)pyrimidine | HCID 4189212 | — |
| Product | HCID 22732377 | HCID 22732377 | — |
Reaction Steps
The title compound was prepared from 4-chloro-6-methyl-2-(3-methylphenyl)pyrimidine (100 mg, 0.457 mmol) and m-anisidine (51 μl, 0.457 mmol) similar to Example 11 as a pale yellow solid (11 mg, 8%). 1H NMR (DMSO-d6): 8.09 (s, 1H), 8.05 (d, J=7.5 Hz, 1H), 7.54–7.49 (m, 4H), 7.35 (t, J=8.1 Hz, 1H), 7.21 (s, 1H), 6.78 (s, 2H), 3.81 (s, 3H), 2.43 (s, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-647381a53d96467d9cbfe6a9e5d3bc9e |
| Source note | uspto-grants-2007_06 |