3-Aminobenzonitrile → HCID 22732384, compound

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Reaction Steps

The title compound was prepared from 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (100 mg, 0.486 mmol) and 3-aminobenzonitrile (57 mg, 0.486 mmol) similar to Example 11 and isolated as a pale white solid (107 mg, 76%). 1H NMR (DMSO-d6): 10.14 (s, 1H), 8.78–8.75 (m, 1H), 8.56 (s, 1H), 8.32 (d, J=7.8 Hz, 1H), 8.04–7.96 (m, 2H), 7.60–7.47 (m, 3H), 6.75 (s, 1H), 2.47 (s, 3H).

Provenance & Evidence