HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isopropylaniline → HCID 9814966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isopropylaniline | HCID 458679 | — |
| Reactant | 4-Chloro-6-methyl-2-(pyridin-2-yl)pyrimidine | HCID 2763395 | — |
| Product | HCID 9814966 | HCID 9814966 | — |
Reaction Steps
The title compound was prepared from a mixture of 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (50 mg, 0.243 mmol) and 3-isopropylaniline (33 μl, 0.243 mmol) similar to Example 13 and isolated as a gray oil (70 mg, 95%). 1H NMR (CDCl3): 8.79–8.77 (m, 1H), 8.47–8.43 (m, 1H), 7.81–7.75 (m, 1H), 7.35–7.25 (m, 3H), 7.17–7.12 (m, 2H), 7.02 (d, J=7.5 Hz, 1H), 2.93–2.84 (m, 1H), 2.45 (s, 3H), 1.24 (d, J=6.9 Hz, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-b92dcb2590ed4ee388103e18b8f23d17 |
| Source note | uspto-grants-2007_06 |