HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyphenol → HCID 22732505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyphenol | HCID 9007 | — |
| Reactant | 4-Chloro-6-methyl-2-(pyridin-2-yl)pyrimidine | HCID 2763395 | — |
| Product | HCID 22732505 | HCID 22732505 | — |
Reaction Steps
The title compound was prepared from a mixture of 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (50 mg, 0.243 mmol) and 3-methoxyphenol (27 μl, 0.243 mmol) similar to Example 13 and isolated as a white oil (24 mg, 34%). 1H NMR (CDCl3): 8.79–8.76 (m, 1H), 8.26–8.23 (m, 1H), 7.75–7.69 (m, 1H), 7.33–7.28 (m, 2H), 6.82–6.72 (m, 3H), 6.58 (s, 1H), 3.77 (s, 3H), 2.58 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-c67d0478856d4b349ef570d51f09575f |
| Source note | uspto-grants-2007_06 |