HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminophenol → HCID 22732425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | 4-Chloro-2-(2-pyrazinyl)-6-(trifluoromethyl)pyrimidine | HCID 22732367 | — |
| Product | HCID 22732425 | HCID 22732425 | — |
Reaction Steps
The title compound was prepared from a mixture of 4-chloro-2-(2-pyrazinyl)-6-(trifluoromethyl)pyrimidine (50 mg, 0.192 mmol) and 3-aminophenol (31 mg, 0.288 mmol) similar to Example 97 and isolated as a tan solid (28 mg,). 1H NMR (DMSO-d6): 10.26 (s, 1H), 9.62 (s, 1H), 9.51–9.50 (m, 1H), 8.87–8.83 (m, 2H), 7.30 (s, 1H), 7.23–7.21 (m, 3H), 6.57–6.54 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226927B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-c647a36bf2ac40e9bd8b223d710b4811 |
| Source note | uspto-grants-2007_06 |