2,5-Dimethoxyaniline → HCID 22732369, compound

Participants

Reaction Steps

The title compound was prepared from a mixture 4-chloro-2,6-di(2-pyridinyl)pyrimidine (25 mg, 0.093 mmol) and 2,5-dimethoxyaniline (21 mg, 0.140 mmol) similar to Example 111 and isolated as a yellow oil (2 mg, 6%). 1H NMR (CDCl3): 8.86–8.84 (m, 1H), 8.70–8.64 (m, 3H), 8.11 (s, 1H), 7.92 (s, 1H), 7.91–7.85 (m, 2H), 7.65 (s, 1H), 7.43–7.36 (m, 2H), 6.87 (d, J=9.0 Hz, 1H), 6.61 (dd, J=3.0, 9.0 Hz, 1H), 3.89 (s, 3H), 3.86 (s, 3H).

Provenance & Evidence