反应详情

The title compound was prepared from a mixture 4-chloro-2,6-di(2-pyridinyl)pyrimidine (25 mg, 0.093 mmol) and 2-methoxy-5-methylaniline (19 mg, 0.140 mmol) similar to Example 111 and isolated as a yellow solid (12 mg, 35%). 1H NMR (CDCl3): 8.89–8.87 (m, 1H), 8.69–8.64 (m, 3H), 7.92–7.84 (m, 3H), 7.89 (s, 1H), 7.55 (s, 1H), 7.44–7.36 (m, 2H), 6.92 (dd, J=1.8, 8.1 Hz, 1H), 6.85 (d, J=8.1 Hz, 1H), 3.86 (s, 3H), 2.39 (s, 3H).