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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1765269Generated: November 1, 2026

3-Phenoxyaniline → HCID 22732520, compound

https://huagongshe.com/reaction/1765269

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-PhenoxyanilineHCID 77135—
Reactant4-Chloro-6-methyl-2-(pyridin-2-yl)pyrimidineHCID 2763395—
ProductHCID 22732520HCID 22732520—

Reaction Steps

The title compound was prepared from 4-chloro-6-methyl-2-(2-pyridinyl)pyrimidine (82.3 mg, 0.4 mmol) and 3-phenoxyaniline (74.0 mg, 0.4 mmol) similar to Example 173 and was isolated as a white solid. (96 mg, 68%). 1H NMR (CDCl3): 8.62 (d, J=4.2 Hz, 1H), 8.25 (d, J=8.1 Hz, 1H), 7.65 (t, J=1.5 Hz, 1H), 7.21 (m, 5H), 6.94 (m, 5H), 6.64 (d, J=8.1 Hz, 1H), 6.49 (s, 1H), 2.33 (s, 3H),

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07226927B2
Source datasetuspto-grants-2007_06
ORD IDord-5f75376990a944b5b8e1ccace74f66e0
Source noteuspto-grants-2007_06