Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 3,5-Diisopropyl-4-methoxybenzaldehyde | HCID 10585025 | — |
| Reactant | HCID 69501695 | HCID 69501695 | — |
| Solvent | Diethylether hexane | HCID 21584099 | — |
| Product | HCID 12133344 | HCID 12133344 | — |
Reaction Steps
Methyl 3-(3,5-diisopropyl-4-methoxyphenyl)acrylate. 3,5-diisopropyl-4-methoxybenzaldehyde (881 mg) free powder. Ph3P═CHCOOCH3 (1.7 g) was added, followed by 10 mL of hexane. The reaction mixture was heated at 50° C. for 24 hours, and the resulting mixture was loaded on a silica-gel column. Chromatography, with diethyl ether:hexane (10:90) as the eluent, provided the ester (944 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07226946B2 |
|---|
| Source dataset | uspto-grants-2007_06 |
|---|
| ORD ID | ord-aaa8edbc24624f5380abcecad7596102 |
|---|
| Source note | uspto-grants-2007_06 |
|---|
