HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → Methyl-4-iodocinnamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 4-Iodocinnamic acid | HCID 3599788 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Methyl-4-iodocinnamate | HCID 582796 | — |
Reaction Steps
A stirred, cooled (ice bath) solution of 4-iodo-cinnamic Acid in methanol was treated with a solution of diazomethane in diethyl ether. The reaction mixture was allowed to warm to ambient temperature, the volatiles were-evaporated in vacuo to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226951B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-885fbbbe44cf4bea960f63f23abe9bbc |
| Source note | uspto-grants-2007_06 |