HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 4-tert-Butyl-2-ethynyl-1-methyl-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (5-Tert-butyl-2-methyl-phenylethynyl)trimethyl-silane | HCID 69070941 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-tert-Butyl-2-ethynyl-1-methyl-benzene | HCID 21107190 | — |
Reaction Steps
Following general procedure F and using (5-tert-butyl-2-methyl-phenylethynyl)-trimethyl-silane (Intermediate 109, 0.16 g, 0.66 mmol), methanol (5 mL) and potassium carbonate (0.05 g, 0.36 mmol), the title compound was obtained (0.08 g, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07226951B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-99fa2b0f3d3a400eaeab435dc07c3beb |
| Source note | uspto-grants-2007_06 |