HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Azobis(cyclohexanecarbonitrile) → Propofol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Azobis(cyclohexanecarbonitrile) | HCID 74978 | — |
| Reactant | HCID 58884383 | HCID 58884383 | — |
| Reactant | HCID 85593397 | HCID 85593397 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Propofol | HCID 4943 | — |
Reaction Steps
The polymerisation carried in a manner similar to that Whitcombe et al. The Molar ratio used was of (2,6-diisopropyl)phenyl (4-vinylphenyl) carbonate to crosslinker (ethylenedimethacrylic acid) to 1,1′-azobis(cyclohexanecarbonitrile) (ABCHC) was 1:19:0.125 for bulk and 1:1:0.125 for membranes, 2 ml/g monomers as porogen (toluene). The polymerisation took 48 hors to complete at 60–80° C. for bulk polymer and 24 hours for the membranes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07229836B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-a226ae32474d4ca1abbe2d3d66ccaf9b |
| Source note | uspto-grants-2007_06 |