HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178525490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 178500540 | HCID 178500540 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178525490 | HCID 178525490 | 78% |
Reaction Steps
Prepared analogously to Example 5 from methyl γ-oxo-1H-benzimidazol-5-butanoate, lithium hydroxide and water in the presence of tetrahydrofuran in a yield of 78% of theoretical. Colourless crystals, m.p. 251–255° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230001B1 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-b7696ed26cf84c32bff03f1bfed22645 |
| Source note | uspto-grants-2007_06 |