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HRID1766224

反应详情

EQUATION

反应方程式

HRID 1766224 的结构方程式

REACTANTS

反应物

2
结构：Cl.c1ccncc1
HCID10176127

Pyridine hydrochloride

C5H6ClN

结构：COc1cc(C)c2c(c1)c(C1CCN(C)CC1)cn2CCc1ccccc1
HCID69435151

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(O)cc2c(C3CCN(C)CC3)cn(CCc3ccccc3)c12
HCID69433520

未命名化合物

PROCEDURE

实验过程

By a method similar to Preparation 8, using 5-methoxy-7-methyl-3-(1-methylpiperdin-4-yl)-1-phenethy-1H-indole (0.288 g) and pyridine hydrochloride (25 g) to afford 0.143 (52%) of the title compound: mass spectrum (ion spray): m/z=349 (M+1); Calculated for C23H28N2O-0.3H2O: C, 78.06; H, 8.15; N, 7.92. Found: C, 78.24; H, 8.18; N, 8.11.

WORKUP

后处理

  1. customBy a method similar to Preparation 8