HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → 7-Methyl-3-(1-methylpiperdin-4-yl)-1-phenethyl-1H-indol-5-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 5-Methoxy-7-methyl-3-(1-methylpiperdin-4-yl)-1-phenethyl-1H-indole | HCID 69435151 | — |
| Product | 7-Methyl-3-(1-methylpiperdin-4-yl)-1-phenethyl-1H-indol-5-ol | HCID 69433520 | — |
Reaction Steps
By a method similar to Preparation 8, using 5-methoxy-7-methyl-3-(1-methylpiperdin-4-yl)-1-phenethy-1H-indole (0.288 g) and pyridine hydrochloride (25 g) to afford 0.143 (52%) of the title compound: mass spectrum (ion spray): m/z=349 (M+1); Calculated for C23H28N2O-0.3H2O: C, 78.06; H, 8.15; N, 7.92. Found: C, 78.24; H, 8.18; N, 8.11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230011B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-a7cc9ecfa6724c8bb5a54f6788271ff3 |
| Source note | uspto-grants-2007_06 |