HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23031175, compound → HCID 23031151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23031175 | HCID 23031175 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23031151 | HCID 23031151 | 98.9% |
Reaction Steps
To a solution of dibenzyl[7-(4-benzyloxy-3-isopropenyl-2-methoxyphenoxy)-6-methylindan-4-yl]amine (7.97 g) in tetrahydrofuran (80 mL) was added 10% Pd/C (4.00 g). The mixture was stirred at room temperature under an atmospheric pressure of hydrogen overnight. The insoluble material was removed by filtration. The filtrate was evaporated under reduced pressure to dryness to give the title compound (4.33 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230031B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-cc69c34861514b92be5b3f20181793be |
| Source note | uspto-grants-2007_06 |