Sodium Hydroxide → HCID 23693670, compound

Participants

Reaction Steps

N-[7-(4-hydroxy-3-isopropylphenoxy)-6-methylindan-4-yl]oxamic acid (2.25 g) was dissolved in ethanol (20 mL). Adding a 1 mol/L aqueous solution of sodium hydroxide (6.09 mL), the mixture was stirred for 5 min. The reaction mixture was evaporated under reduced pressure to dryness. Adding water (0.115 mL) and diisopropyl ether (20 mL), the residue was stirred for 3 hours. The precipitate was filtrated to give the title compound (2.4 g).

Provenance & Evidence