HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 17862517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | HCID 69143608 | HCID 69143608 | — |
| Product | HCID 17862517 | HCID 17862517 | 116.4% |
Reaction Steps
According to a similar procedure to that described in Example 1-(11), allyl 2-acetoxy-5-[(4-methoxybenzyl)oxy]-5-oxopentanoate (1.36 g, 3.88 mmol) obtained from Example 2-(3), anisole (1.50 g, 13.87 mmol), and trifluoroacetic acid (3 ml) were reacted, and the reaction mixture was worked up to afford the title compound (1.04 g, quantitative yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07230023B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-5e1daac0463447f782984959a434d10a |
| Source note | uspto-grants-2007_06 |