Oxalyl chloride → HCID 17862488, compound

Participants

Reaction Steps

According to a similar procedure to that described in Example 1-(12), 4-acetoxy-5-allyloxy-5-oxopentanoic acid (345.3 mg, 1.50 mmol) obtained from Example 2-(4) and oxalyl chloride (209.4 mg, 1.65 mmol) were reacted, and the reaction mixture was worked up to afford 4-acetoxy-5-allyloxy-5-oxopentanoyl chloride as a crude product.

Provenance & Evidence