Oxalyl chloride → HCID 17862488, compound

HRID 1766864Notes

Reaction equation

[C:1]([O:4][CH:5]([C:11]([O:13][CH2:14][CH:15]=[CH2:16])=[O:12])[CH2:6][CH2:7][C:8](O)=[O:9])(=[O:3])[CH3:2].C(Cl)(=O)C([Cl:20])=O>>[C:1]([O:4][CH:5]([C:11]([O:13][CH2:14][CH:15]=[CH2:16])=[O:12])[CH2:6][CH2:7][C:8]([Cl:20])=[O:9])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 65578Oxalyl chloride

HCID 17862517HCID 17862517, compound

Product 1

HCID 17862488HCID 17862488, compound

Procedure

According to a similar procedure to that described in Example 1-(12), 4-acetoxy-5-allyloxy-5-oxopentanoic acid (345.3 mg, 1.50 mmol) obtained from Example 2-(4) and oxalyl chloride (209.4 mg, 1.65 mmol) were reacted, and the reaction mixture was worked up to afford 4-acetoxy-5-allyloxy-5-oxopentanoyl chloride as a crude product.

Sources & evidence

ORD record: ord-27c84691d17c461e927f5a2b8246f778
Source dataset: uspto-grants-2007_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07230023B2

Reaction notes

Loading…