HCID 58677164, compound → HCID 21113154, compound

Participants

Reaction Steps

The carbamate (c) (0.93 g, 2.4 mmol) was dissolved in trifluoroacetic acid (40 mL). After 1 hour the mixture was evaporated and the residue partitioned between ethyl acetate and aqueous sodium bicarbonate solution. The organic extract was washed with brine, dried and evaporated affording a solid (2.17 g, 90%).

Provenance & Evidence