HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 135830901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 3-(4-pyridyl)-3-oxopropionate | HCID 2735202 | — |
| Reactant | HCID 17851068 | HCID 17851068 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 135830901 | HCID 135830901 | — |
Reaction Steps
A mixture of 8.98 g (46.5 mmol) of ethyl 3-(4-pyridyl)-3-oxopropionate and 8.0 g (46.5 mmol) of 2-amino-3,4,5,6-tetrahydropyrimidine dihydrochloride (prepared according to J. Org. Chem. 1955, 20, 829) and 19.3 g (139.5 mmol) of potassium carbonate in 60 ml of ethanol was heated at reflux temperature during 18 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07232827B2 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-de806a1e06e0465ab764d479b51e6f5a |
| Source note | uspto-grants-2007_06 |