Benzoic acid, 2-amino-5-iodo- → HCID 23030470, compound

Participants

Reaction Steps

In a 200 mL volume glass vessel equipped with a stirrer and a thermometer were placed 10.0 g (38 mmol) of 5-iodoanthranilic acid and 100 mL (780 mmol) of 15 wt. % ammonia methanol solution. The reaction was carried out for 3 hours at room temperature. After the reaction was complete, the reaction mixture was concentrated under reduced pressure, to obtain 9.0 g (isolated yield: 85%) of ammonium 5-iodoanthranilate as pale red solid.

Provenance & Evidence