huagongshe.com
HRID1767983

反应详情

EQUATION

反应方程式

HRID 1767983 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)[Si](C)(C)Cl
HCID28928

Chloro(1,1-dimethylethyl)dimethylsilane

C6H15ClSi

结构：O=C1CCC(=O)N1Br
HCID67184

1-Bromopyrrolidine-2,5-dione

C4H4BrNO2

结构：CC(C)(C)[Si](C)(C)Oc1ccc2cc[nH]c2c1
HCID22250816

6-{[tert-Butyl(dimethyl)silyl]oxy}-1H-indole

C14H21NOSi

PRODUCTS

生成物

1
结构：CC(C)(C)[Si](C)(C)Oc1ccc2c(Br)cn([Si](C)(C)C(C)(C)C)c2c1
HCID23614490

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 27 b], 6-(tert-butyl-dimethyl-silanyloxy)-1H-indole was reacted with tert-butyldimethylsilyl chloride and subsequently with N-bromosuccinimide to obtain 3-bromo-1-(tert-butyl-dimethyl-silanyl)-6-(tert-butyl-dimethyl-silanyloxy)-1H-indole as brown solid.