Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 69411198 | HCID 69411198 | — |
| Solvent | 9-Borabicyclo(3.3.1)nonane | HCID 78966 | — |
| Product | HCID 11710114 | HCID 11710114 | — |
Reaction Steps
8.0 g (20 mmol) of phosphine oxide (9) were dissolved under an argon atmosphere in 50 ml of 0.5 M THF solution of 9-BBN (Aldrich) and the reaction mixture was heated to 70° C. in a closed reaction vessel for 12 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07235696B2 |
|---|
| Source dataset | uspto-grants-2007_06 |
|---|
| ORD ID | ord-82ee6497930e47c2a7fc3dec1e0dceda |
|---|
| Source note | uspto-grants-2007_06 |
|---|
